bis(3-Methoxyphenyl)aMine

Name: bis(3-Methoxyphenyl)aMine
Brand: Zhengzhou Whchem

CAS：92248-06-1 | bis(3-Methoxyphenyl)aMine | Whchem

CAS: 92248-06-1

Other Names

bis(3-Methoxyphenyl)aMine;Benzenamine, 3-methoxy-N-(3-methoxyphenyl)-;3-Methoxy-N-(3-methoxyphenyl)aniline;bis(3-Methoxyphenyl)aMine ISO 9001：2015 REACH

Molecular Formula

Purity

>97%

Molecular Weight

229.27 g/mol

EINECS

Structure Available Verified Product

English Name	bis(3-Methoxyphenyl)aMine
English Synonyms	bis(3-Methoxyphenyl)aMine;Benzenamine, 3-methoxy-N-(3-methoxyphenyl)-;3-Methoxy-N-(3-methoxyphenyl)aniline;bis(3-Methoxyphenyl)aMine ISO 9001：2015 REACH
CAS Number	92248-06-1
Molecular Formula	C14H15NO2
Molecular Weight	229.27 g/mol
EINECS Number
Related Categories
Mol File	Download MOL File
Structure Image

Property	Value
Boiling point	175-178 °C (Press: 0.8 Torr)
Density	1.126±0.06 g/cm³ (Predicted)
Storage condition	Keep in dark place, Inert atmosphere, Room temperature
Acidity Coefficient (pKa)	0.14±0.50 (Predicted)

bis(3-Methoxyphenyl)aMine (CAS 92248-06-1) is a high-purity fine chemical intermediate widely used in organic synthesis, pharmaceutical R&D, agrochemical manufacturing and specialty chemical applications.

As a professional supplier, Zhengzhou Whchem provides bis(3-Methoxyphenyl)aMine with >97% purity, COA, structure confirmation and flexible packaging, available from research quantities to commercial scale with global shipping.

Category	Description (English Translation)
Uses & Synthesis Methods Production Method: Starting Materials: 10365-98-7 (3-Methoxyphenylboronic acid) 536-90-3 (m-Anisidine) 92248-06-1 (Bis(3-methoxyphenyl)amine) General procedure for the synthesis of bis(3-methoxyphenyl)amine from 3-methoxyphenylboronic acid and m-anisidine: 1. Under nitrogen atmosphere, copper(II) acetate (2.1 mmol) and pyridine (0.25 mL) were added to a vigorously stirred solution of 3-methoxyaniline (1 mmol) and 3-methoxyphenylboronic acid (2 mmol) in anhydrous dichloromethane (3.5 mL). 2. The reaction mixture was stirred at room temperature for 72 hours, and the progress was monitored by thin-layer chromatography (TLC). 3. After completion, the crude reaction mixture was pre-adsorbed onto silica gel and purified by flash column chromatography to afford the target product, bis(3-methoxyphenyl)amine (3c). 4. Product yield: 25%; EI-MS m/z: 229 (M⁺) [Reference: Urgaonkar, S.; Verkade, J.G. J. Org. Chem. 2004, 69, 9135-9142]. References: [1] Patent: WO2007/79593, 2007, A1. Location in patent: Page/Page column 31

Category

Description (English Translation)

Uses & Synthesis Methods

Production Method:

Starting Materials:
10365-98-7 (3-Methoxyphenylboronic acid)
536-90-3 (m-Anisidine)
92248-06-1 (Bis(3-methoxyphenyl)amine)

General procedure for the synthesis of bis(3-methoxyphenyl)amine from 3-methoxyphenylboronic acid and m-anisidine:

1. Under nitrogen atmosphere, copper(II) acetate (2.1 mmol) and pyridine (0.25 mL) were added to a vigorously stirred solution of 3-methoxyaniline (1 mmol) and 3-methoxyphenylboronic acid (2 mmol) in anhydrous dichloromethane (3.5 mL).

2. The reaction mixture was stirred at room temperature for 72 hours, and the progress was monitored by thin-layer chromatography (TLC).

3. After completion, the crude reaction mixture was pre-adsorbed onto silica gel and purified by flash column chromatography to afford the target product, bis(3-methoxyphenyl)amine (3c).

4. Product yield: 25%; EI-MS m/z: 229 (M⁺) [Reference: Urgaonkar, S.; Verkade, J.G. J. Org. Chem. 2004, 69, 9135-9142].

References:
[1] Patent: WO2007/79593, 2007, A1. Location in patent: Page/Page column 31

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bis(3-Methoxyphenyl)aMine

CAS：92248-06-1 | bis(3-Methoxyphenyl)aMine | Whchem

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